1. Beamline
12-ID Overview
2. Sample
Holders
A. Standard
Capillary Holder
Hole
Size: Capillary diameter 1.0 - 2.0
mm; also have stripes good for NMR tube 5.0 mm
Side View
Top View
B. Static Transmission SAXS Sample Mounting Frame
C. GISAXS/GIWAXS Sample Holders
- Single
and multiple samples holders are available for GISAXS/WAXS
measurements. In additional to theta alignment, chi and phi alignment
also available at 12-ID-B.
Single
sample holder with chi alignment
Multiple sample holder with phi motion
3. Sample Heaters
A. Linkam THMS600 Stage and Accessories
 
Linkam THMS600
T-Zero Press
B. Multi-Sample
Heater for Capillary and DSC pan samples.
Front View
Top View
 
Dimensions
and Drawings of Multi-Sample Heater Pieces:
1.
Capillary Holder
2. DSC Pan
Holder. This cell is designed for a DSC cell, but
any solid can be filled in and covered up with Kapton tape on both
sides.
C. Water bath with
computer contol.
4. Solution Sample
Instruments and Devivces
- Flow Cells.
Multiple flow cells are being used at 12-ID-B for solution samples,
especially for biomacromolecular samples. Below shows the flow cell
assemblies for room temperature and varied temperature meausrements.
Room
Temperature Flow Cell
Flow
Cell with Temperature
Control ( 4 - 80 C)
- Syringe Pumps.
A few types of syringe pumps are available at 12-ID-B. All of them can
be either programmed or computer-controlled.
Haminton
microlab 600
Multiple-valve
syringe pump
- SEC-SAXS at 12-ID-B.
An AKTA micro FPLC is employed at 12-ID-B for SEC-SAXS measurement.
AKTA FPLC
SEC-SAXS at 12-ID-B
5. Other Devices
Eppendorf
Microcentrifuge for small tubes (1.5mL) and Biofuge Primo R centrifuge
for large tube(15mL and 50mL) are available in wet-lab.
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