Size: Capillary diameter 1.0 - 2.0
mm; also have stripes good for NMR tube 5.0 mm
B. Static Transmission SAXS Sample Mounting Frame
C. GISAXS/GIWAXS Sample Holders
and multiple samples holders are available for GISAXS/WAXS
measurements. In additional to theta alignment, chi and phi alignment
also available at 12-ID-B.
sample holder with chi alignment
Multiple sample holder with phi motion
3. Sample Heaters
A. Linkam THMS600 Stage and Accessories
Heater for Capillary and DSC pan samples.
and Drawings of Multi-Sample Heater Pieces:
2. DSC Pan
Holder. This cell is designed for a DSC cell, but
any solid can be filled in and covered up with Kapton tape on both
C. Water bath with
4. Solution Sample
Instruments and Devivces
- Flow Cells.
Multiple flow cells are being used at 12-ID-B for solution samples,
especially for biomacromolecular samples. Below shows the flow cell
assemblies for room temperature and varied temperature meausrements.
Temperature Flow Cell
Cell with Temperature
Control ( 4 - 80 C)
- Syringe Pumps.
A few types of syringe pumps are available at 12-ID-B. All of them can
be either programmed or computer-controlled.
- SEC-SAXS at 12-ID-B.
An AKTA micro FPLC is employed at 12-ID-B for SEC-SAXS measurement.
SEC-SAXS at 12-ID-B
5. Other Devices
Microcentrifuge for small tubes (1.5mL) and Biofuge Primo R centrifuge
for large tube(15mL and 50mL) are available in wet-lab.